Thermally formed oxide films on Al-6Zn-XMg (X 5 0 and 2 mass%) alloys heated in different gases

Po Chen Chen; Teng Shih Shih; Juen Shiou Chen

doi:10.1007/s10973-009-0088-2

Thermally formed oxide films on Al-6Zn-XMg (X 5 0 and 2 mass%) alloys heated in different gases

Po Chen Chen, Teng Shih Shih, Juen Shiou Chen

機械工程學系

研究成果: 雜誌貢獻 › 期刊論文 › 同行評審

1 引文斯高帕斯（Scopus）

摘要

In this study, thermogravimetric analysis (TG) testing is used to measure the mass loss of polished Al-6Zn-XMg (X = 0 and 2 mass%) alloy samples heated at 773 K for 6 h in dry air or nitrogen gas. The progressive development of thermally formed oxides on an Al-6Zn-XMg(X = 0 and 2 mass%) alloy as shown by X-ray diffractometer analyses is discussed. Zn-spinel and Mg-spinel are detected on the Al-6Zn and Al-6Zn-2Mg alloy samples, respectively, and then heated in the dry air atmosphere; AlN and Mg₃N₂ are detected in alloy samples heated in nitrogen gas. The chain reactions that cause the serrated change in the mass loss curve are proposed and discussed.

原文	???core.languages.en_GB???
頁（從 - 到）	229-235
頁數	7
期刊	Journal of Thermal Analysis and Calorimetry
卷	99
發行號	1
DOIs	https://doi.org/10.1007/s10973-009-0088-2
出版狀態	已出版 - 1月 2010

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10.1007/s10973-009-0088-2

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@article{2e628fca2b7f461aa949568ec74da5d7,

title = "Thermally formed oxide films on Al-6Zn-XMg (X 5 0 and 2 mass\%) alloys heated in different gases",

abstract = "In this study, thermogravimetric analysis (TG) testing is used to measure the mass loss of polished Al-6Zn-XMg (X = 0 and 2 mass\%) alloy samples heated at 773 K for 6 h in dry air or nitrogen gas. The progressive development of thermally formed oxides on an Al-6Zn-XMg(X = 0 and 2 mass\%) alloy as shown by X-ray diffractometer analyses is discussed. Zn-spinel and Mg-spinel are detected on the Al-6Zn and Al-6Zn-2Mg alloy samples, respectively, and then heated in the dry air atmosphere; AlN and Mg3N2 are detected in alloy samples heated in nitrogen gas. The chain reactions that cause the serrated change in the mass loss curve are proposed and discussed.",

keywords = "AlN, MgN, Spinel, TG, XRD",

author = "Chen, \{Po Chen\} and Shih, \{Teng Shih\} and Chen, \{Juen Shiou\}",

note = "Funding Information: Acknowledgements The authors would like to thank the National Science Council of Taiwan for providing financial support for this study under Grant Number NSC97-2221-E-008-017.",

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doi = "10.1007/s10973-009-0088-2",

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TY - JOUR

T1 - Thermally formed oxide films on Al-6Zn-XMg (X 5 0 and 2 mass%) alloys heated in different gases

AU - Chen, Po Chen

AU - Shih, Teng Shih

AU - Chen, Juen Shiou

N1 - Funding Information: Acknowledgements The authors would like to thank the National Science Council of Taiwan for providing financial support for this study under Grant Number NSC97-2221-E-008-017.

PY - 2010/1

Y1 - 2010/1

N2 - In this study, thermogravimetric analysis (TG) testing is used to measure the mass loss of polished Al-6Zn-XMg (X = 0 and 2 mass%) alloy samples heated at 773 K for 6 h in dry air or nitrogen gas. The progressive development of thermally formed oxides on an Al-6Zn-XMg(X = 0 and 2 mass%) alloy as shown by X-ray diffractometer analyses is discussed. Zn-spinel and Mg-spinel are detected on the Al-6Zn and Al-6Zn-2Mg alloy samples, respectively, and then heated in the dry air atmosphere; AlN and Mg3N2 are detected in alloy samples heated in nitrogen gas. The chain reactions that cause the serrated change in the mass loss curve are proposed and discussed.

AB - In this study, thermogravimetric analysis (TG) testing is used to measure the mass loss of polished Al-6Zn-XMg (X = 0 and 2 mass%) alloy samples heated at 773 K for 6 h in dry air or nitrogen gas. The progressive development of thermally formed oxides on an Al-6Zn-XMg(X = 0 and 2 mass%) alloy as shown by X-ray diffractometer analyses is discussed. Zn-spinel and Mg-spinel are detected on the Al-6Zn and Al-6Zn-2Mg alloy samples, respectively, and then heated in the dry air atmosphere; AlN and Mg3N2 are detected in alloy samples heated in nitrogen gas. The chain reactions that cause the serrated change in the mass loss curve are proposed and discussed.

KW - AlN

KW - MgN

KW - Spinel

KW - TG

KW - XRD

UR - https://www.scopus.com/pages/publications/77951667693

U2 - 10.1007/s10973-009-0088-2

DO - 10.1007/s10973-009-0088-2

M3 - 期刊論文

AN - SCOPUS:77951667693

SN - 1388-6150

VL - 99

SP - 229

EP - 235

JO - Journal of Thermal Analysis and Calorimetry

JF - Journal of Thermal Analysis and Calorimetry

IS - 1

ER -

Thermally formed oxide films on Al-6Zn-XMg (X 5 0 and 2 mass%) alloys heated in different gases

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