Simplified derivatization method for triclosan determination in personal care products by gas chromatography-mass spectrometry

Chiao Yin Cheng; Yu Chen Wang; Hsin Chang Chen; Wang Hsien Ding

doi:10.1002/jccs.201190057

Simplified derivatization method for triclosan determination in personal care products by gas chromatography-mass spectrometry

Chiao Yin Cheng, Yu Chen Wang, Hsin Chang Chen, Wang Hsien Ding

化學學系

研究成果: 雜誌貢獻 › 期刊論文 › 同行評審

8 引文斯高帕斯（Scopus）

摘要

An efficient and eco-friendly injection-port tert-butyldimethylsilylated (TBDMS) derivatization and gas chromatography-mass spectrometry (GC-MS) was developed to determine triclosan (TCS, an antibacterial agent) in the samples of toothpaste, liquid hand-soap and facial cleansing cream. This on-line derivatization coupled ultrasonic extraction provides sensitivity, fast and reproducible results for TCS analysis. The accuracy and precision of the method was evaluated. The developed method was successfully applied to determine the content of TCS in selected personal care products.

原文	???core.languages.en_GB???
頁（從 - 到）	49-52
頁數	4
期刊	Journal of the Chinese Chemical Society
卷	58
發行號	1
DOIs	https://doi.org/10.1002/jccs.201190057
出版狀態	已出版 - 2月 2011

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10.1002/jccs.201190057

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title = "Simplified derivatization method for triclosan determination in personal care products by gas chromatography-mass spectrometry",

abstract = "An efficient and eco-friendly injection-port tert-butyldimethylsilylated (TBDMS) derivatization and gas chromatography-mass spectrometry (GC-MS) was developed to determine triclosan (TCS, an antibacterial agent) in the samples of toothpaste, liquid hand-soap and facial cleansing cream. This on-line derivatization coupled ultrasonic extraction provides sensitivity, fast and reproducible results for TCS analysis. The accuracy and precision of the method was evaluated. The developed method was successfully applied to determine the content of TCS in selected personal care products.",

keywords = "GC-MS, Injection-port derivatization, Personal care products analysis, Triclosan",

author = "Cheng, {Chiao Yin} and Wang, {Yu Chen} and Chen, {Hsin Chang} and Ding, {Wang Hsien}",

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T1 - Simplified derivatization method for triclosan determination in personal care products by gas chromatography-mass spectrometry

AU - Cheng, Chiao Yin

AU - Wang, Yu Chen

AU - Chen, Hsin Chang

AU - Ding, Wang Hsien

PY - 2011/2

Y1 - 2011/2

N2 - An efficient and eco-friendly injection-port tert-butyldimethylsilylated (TBDMS) derivatization and gas chromatography-mass spectrometry (GC-MS) was developed to determine triclosan (TCS, an antibacterial agent) in the samples of toothpaste, liquid hand-soap and facial cleansing cream. This on-line derivatization coupled ultrasonic extraction provides sensitivity, fast and reproducible results for TCS analysis. The accuracy and precision of the method was evaluated. The developed method was successfully applied to determine the content of TCS in selected personal care products.

AB - An efficient and eco-friendly injection-port tert-butyldimethylsilylated (TBDMS) derivatization and gas chromatography-mass spectrometry (GC-MS) was developed to determine triclosan (TCS, an antibacterial agent) in the samples of toothpaste, liquid hand-soap and facial cleansing cream. This on-line derivatization coupled ultrasonic extraction provides sensitivity, fast and reproducible results for TCS analysis. The accuracy and precision of the method was evaluated. The developed method was successfully applied to determine the content of TCS in selected personal care products.

KW - GC-MS

KW - Injection-port derivatization

KW - Personal care products analysis

KW - Triclosan

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M3 - 期刊論文

AN - SCOPUS:79955546434

SN - 0009-4536

VL - 58

SP - 49

EP - 52

JO - Journal of the Chinese Chemical Society

JF - Journal of the Chinese Chemical Society

IS - 1

ER -

Simplified derivatization method for triclosan determination in personal care products by gas chromatography-mass spectrometry

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